תיאור
These 4550 Reactors extend the size range of the 4530 Series to 1 and 2 gallon (3.75 and 7.5 liter) sizes, providing excellent facilities for pilot plant studies. They can be furnished with either a self-sealing O-ring closure for working temperatures up to 225 °C, or with a flat, PTFE gasket for higher temperatures to 350 °C. Both fixed head and moveable head designs are available. The moveable head, Model 4551 and 4552, reactors are designed so that they can be opened or closed conveniently without removing the cylinder from the heater and without auxiliary handling equipment. The split-ring cover clamp sections can be moved into place from the sides, and the cap screws can be tightened with the vessel in place in its heater. The fixed head versions, Model 4553 and 4554, allow the head (and the connections made to it) to remain in place while the cylinder and heater are lowered with the aid of the included pneumatic lift system.
The 1 gallon size is usually recommended for high viscosity polymer studies. An optional bottom drain valve may be added for convenient product recovery. As with the smaller floor stand models, these larger, self-contained systems can be equipped with a variety of attachments, such as: condensers, solids charging port, bottom drain, special motors, special heaters, jacketed vessels and automatic valves and regulators. Because of the higher wattage heaters for these reactors, all models in the 4550 Series require a 230 volt power supply.
Model Number | 4551 | 4552 | 4553 | 4554 |
Approximate Volume, mL | 1 (3.75) | 2 (7.99) | 1 (3.75) | 2 (7.99) |
Maximum Pressure (MAWP) | 1900 psi (131 bar) | |||
Maximum Temperature | ||||
with FKM O-ring | 225 °C | |||
with FFKM O-ring | 300 °C | |||
with PTFE Flat Gasket | 350 °C | |||
Reactor Details | ||||
Mounting Style | Moveable | Fixed Head | ||
Stand Type | Cart | Floor Stand | ||
Closure | Split-Ring (10 Compression Bolts for Flat Gasket, no Compression Bolts for O-ring) |
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Valve Connections | 1/4″ Male NPT | |||
Magnetic Drive, Model No. | A1180HC General Purpose or A2160HC Footless | |||
Maximum Torque | 60 Inch-Pounds | |||
Impeller(s), 6 blades | 2 (3.85″ dia.) | |||
Stirrer Motor | 1/2 hp variable speed | |||
Pressure Gage, Size | 4.5 inches | |||
Range | 0 – 2000 psi (138 bar) | |||
Temperature Measurement | Thermowell | |||
Cooling Coil (optional) | Serpentine | |||
Bottom Drain Valve (BDV) (optional) | 3/8″ NPT | |||
Lift Mechanism (optional) | N/A | Pneumatic | ||
Heater Style | Calrod | |||
Heater Power, Watts | 2250 | 2700 | 2250 | 2700 |
Electrical Supply | ||||
Volts, AC | 230 | |||
Maximum Load, amps, 230 | 13 | 15 | 13 | 15 |
Cylinder Dimensions | ||||
I.D. x Depth, inches | 6.0 x 8.6 | 6.0 x 17.2 | 6.0 x 8.6 | 6.0 x 17.2 |
Vessel Assembly Weight, pounds | 96 | 116 | 111 | 131 |
Cylinder Weight, pounds | 33 | 52 | 33 | 52 |
Reactor/Stand Dimensions | ||||
Width x Depth, inches w/o Controller | 35 x 18 | 20 x 31 | ||
Height, inches | 50 | 75 | ||
Weight, pounds | 265 | 295 | 315 | 343 |
Spare Parts Kit | 4559M |