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FT-IR – Coupling for Fourier-Transform Infrared spectrometer. Netzsch, Germany

More than just the sum of its parts

Especially in the polymer field as well as in the pharmaceutical and chemical industries, it can be very useful to have knowledge about the gases that evolve during a process, curing/cross-linking, decomposition or any other reaction.
With the vacuum-tight thermal balances and simultaneous thermal analysis instruments TG 209 F1 Libra®TG/STA 449 F3 Jupiter® and TG/STA 449 F1Jupiter®TG/STA 449 F5 Jupiter®STA 2500 RegulusDIL 402 Expedis Select & Supreme, and TMA 402 F1/F3 Hyperion®, as well as with the dynamic differential calorimeters DSC 404 F1 Pegasus® and DSC 204 F1 Phoenix®, NETZSCH offers you efficient systems for coupling to a Fourier Transform Infrared Spectrometer (FT-IR). The transfer line and the connection adaptors to the furnaces can be heated up to 230°C to prevent condensation of the decomposition products to the greatest extent possible. For spectra interpretation, extensive gas phase libraries are available.

תיאור

The FT-IR coupling can be employed for the following application areas:

  • Decomposition
  • Dehydration
  • Residual solvent content
  • Pyrolysis
  • Solid-gas reactions
  • Combustion
  • Oxidation
  • Corrosion
  • Catalysis
  • Compositional analysis
  • Binder burn-out
  • Coal analysis
  • Polymer content
  • Ash content
  • Evaporation, outgassing

 

Key Technical Data

  • Wave number range: 
    FT-IR: 8000 cm-1 to 340 cm-1
    Coupling: 4400 cm-1 to 600 cm-1
    (double window technique KBr+ZnSe)
  • Resolution: 
    better than 0.4 cm-1
  • Temperature of transfer line: 
    max. 230°C
  • Furnace adaptor: 
    max. 300°C
  • Transfer line material: 
    PTFE (exchangeable)
  • Window material gas cell: 
    ZnSe + KBr
  • Gas cell volume and length: 
    8.7 ml/110 mm
  • Detector: 
    DLaTGS or MCT
schematics of FT-IR coupling

 

Software

 

The FT-IR coupling runs under OPUS and  Proteus® software on Windows®Proteus® includes everything you need to carry out a measurement and evaluate the resulting data. Easy-to-understand menus and automated routines make Proteus® extremely user-friendly while still allowing for sophisticated analysis. Proteus®software is licensed with the instrument and can of course be installed on other computer systems.

 

Features:

  • Simultaneous measuring, data acquisition, and data storage with the two software packages: Proteus® (NETZSCH) for thermal analysis data, and OPUS (Bruker Optics) for FT-IR spectra and traces
  • OPUS/CHROM software as 2D and 3D plots for FT-IR and TG/STA/DSC measuring curves as functions of time and temperature
  • OPUS/SEARCH with spectra library
  • Traces for evaluation of characteristic temperatures and peak area together with thermal analysis curves
  • Gram-Schmidt plot with temperature and peak area calculation together with thermal analysis curves

 

השאירו לנו הודעה

שירות טכני: 08-683-6306
מכירות: 072-395-0508
מייל: info@medent.co.il

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